Synthesis of 7-substituted 3-aminothieno[2,3-d:4,5-d′]-dipyrimidin-4(3H)-ones
✍ Scribed by S. P. Tumkyavichyus
- Publisher
- Springer US
- Year
- 1988
- Tongue
- English
- Weight
- 380 KB
- Volume
- 24
- Category
- Article
- ISSN
- 0009-3122
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📜 SIMILAR VOLUMES
The asymmetric unit of the title compound, C 19 H 16 FN 5 O 4 , contains two independent molecules. The dihedral angles between the main planes and the fluorophenyl rings in the two molecules are 83.24 (5) and 71.76 (4) . Weakstacking interactions may be effective in the stabilization of the crystal
## Abstract magnified image The thienopyridine derivative **2**, obtained from reaction of acetoacetic ester with **1** in the presence of tin tetrachloride, was treated with triphenylphosphine in hexachloroethane and Et~3~N to give iminophosphorane **3**. Iminophosphorane **3** reacted with pheny