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Synthesis of 6-Hydroxy-2-methyl-3-thioxo-2H-1,2,4-triazin-5-one

✍ Scribed by Branch, Clive L.; Eggleston, Drake S.; Haltiwanger, R. Curtis; Kaura, Arun C.; Tyler, John W.

Book ID
111871406
Publisher
Taylor and Francis Group
Year
1996
Tongue
English
Weight
316 KB
Volume
26
Category
Article
ISSN
0039-7911

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The title compound, C 14 H 16 N 2 O 4 S, was synthesized by the reaction of 4-hydroxy-3-methoxybenzaldehyde, thiourea and methyl 3-oxobutanoate in ethanol under reflux. The crystal structure is stabilized mainly through intermolecular N-HÁ Á ÁS and O-HÁ Á ÁO hydrogen bonds. The tetrahydropyrimidin-2