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Synthesis of 5-formyl-2′-deoxyuridine and the α-anomer

✍ Scribed by Mathias P. Mertes; Mohammed T. Shipchandler

Book ID
112122204
Publisher
Journal of Heterocyclic Chemistry
Year
1970
Tongue
English
Weight
94 KB
Volume
7
Category
Article
ISSN
0022-152X

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Synthesis of 5-deuteromethyl-2′-deoxyuridine (thymidine-α,α,α-d3) and related compounds
✍ C.-Y. Shiue; A. P. Wolf; D. N. Slatkin 📂 Article 📅 1980 🏛 John Wiley and Sons 🌐 French ⚖ 289 KB

## Abstract Thymine‐α,α,α‐d~3~ (**4**) was synthesized from perdeuterated methyl iodide and pyrimidine‐lithium. Thymidine‐α,α,α‐d~3~ (**8**) was then synthesized by coupling compound **4** with 1α‐chloro‐2‐deoxy‐3,5‐bis(p‐toluoyl)‐α‐D‐ribofuranosyl chloride in the presence of Friedal‐Crafts catalys