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Synthesis of 4,4′-dichloro-3,5,3′,5′-tetramethylbiphenyl by the sandmeyer reaction

✍ Scribed by P.David Josephy; Marie Weerasooriya

Book ID
118026418
Publisher
Elsevier Science
Year
1983
Tongue
English
Weight
110 KB
Volume
12
Category
Article
ISSN
0045-6535

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## Abstract [^14^C] Aniline hydrogen sulphate was acetylated, and the acetanilide obtained was chlorinated with N‐chlorosuccinimide to 2‐chloro, 4‐chloro‐ and 2, 4‐dichloroacet[^14^C] anilide. The labelled 2‐ and 4‐chloroacet[^14^C] anilides were hydrolyzed and treated with aluminium chloride, hydr