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Synthesis of 4-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-1,6-anhydro-3-O-(4-methoxybenzoyl)-β- D-mannopyranose: A versatile intermediate for the preparation of N,N-diacetylchitobiose derivatives

✍ Scribed by M. Kloosterman; P. Westerduin; J. H. van Boom


Publisher
Elsevier Science
Year
2010
Tongue
English
Weight
409 KB
Volume
105
Category
Article
ISSN
0165-0513

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✍ Färnbäck, Magnus ;Söderman, Peter ;Eriksson, Lars ;Widmalm, Göran 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 661 KB

The title compound, C 51 H 56 N 4 O 21 Á0.1C 6 H 14 , crystallizes with two independent protected trisaccharide molecules and a partially occupied hexane solvent molecule in the asymmetric unit. The major conformational difference between the two trisaccharide molecules involves the O-acetyl group a