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Synthesis of 4-alkoxy-4-methyl- and 4-alkoxy-4-fluoromethyl-1,3-benzoxazinones

✍ Scribed by Hamad Z Alkhathlan


Book ID
108282359
Publisher
Elsevier Science
Year
2003
Tongue
French
Weight
226 KB
Volume
59
Category
Article
ISSN
0040-4020

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4-Alkoxy-3β€²-(alkylthio)-3,4β€²-diquinoliny
✍ Andrzej MaΕ›lankiewicz; Stanistaw Boryczka πŸ“‚ Article πŸ“… 2010 πŸ› Elsevier Science 🌐 English βš– 638 KB

## Abstract The reactions of thioquinanthrene (1) with sodium alkoxides derived from 23 alcohols followed by S‐alkylation gave the title 4‐alkoxy‐3′‐(alkylthio)‐3,4′‐diquinolinyl sulfides 3 (18.5–91.5%) and, in some cases, 1,4‐dihydro‐4‐oxo‐3′‐(alkylthio)‐3,4′‐diquinolinyl sulfides 4a (up to 31.5%)