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Synthesis of (±)-4-alkanolides from pent-4-enoic acid

✍ Scribed by T. M. Ugurchieva; A. V. Lozanova; M. V. Zlokazov; V. V. Veselovsky

Book ID
106520840
Publisher
Springer
Year
2008
Tongue
English
Weight
245 KB
Volume
57
Category
Article
ISSN
1573-9171

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Regioselective synthesis of (E)-2-[2H or 3H]-5-succinimido-4-oxo-pent-2-enoic acid
✍ Arie L. Gutman; John B. Campbell 📂 Article 📅 1985 🏛 John Wiley and Sons 🌐 French ⚖ 295 KB

## Abstract The synthesis of highly enriched C‐2 deuteriated and tritiated (E)‐5‐succinimido‐4‐oxo‐pent‐2‐enoic acid for use in enzymatic reduction is described. The starting materials 3‐methoxycarbonyl‐[3‐^2^H]propionyl chloride and 3‐methoxycarbonyl‐[3‐^3^H]propionyl chloride were prepared in hig