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Synthesis of (±) 3,6-di-O-benzyl-2-myo-inosose 1,4,5-tri-O-dibenzylphosphate as potential intermediate for the preparation of tritium-labelled myo-inositol 1,4,5-triphosphate

✍ Scribed by Nathalie Schnetz-Boutaud; Bernard Spiess; Gilbert Schlewer

Publisher: Elsevier Science
Year: 1994
Tongue: English
Weight: 423 KB
Volume: 259
Category: Article
ISSN: 0008-6215
DOI: 10.1016/0008-6215(94)84204-3

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## Abstract Variable‐temperature ^13^C CP/MAS NMR experiments were carried out on crystalline (±)‐3,4‐di‐__O__‐acetyl‐1,2,5,6‐tetra‐__O__‐benzyl‐__myo__‐inositol. Three distinct phases can be distinguished from their NMR characteristics, each stable over a well defined temperature range, in accord