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Synthesis of 3,4,5-Tris(alkyloxy)benzyl Glycosides and Glycolipid Analogues.

✍ Scribed by Reiko Sato; Kazunori Toma; Kazufumi Nomura; Mutsumi Takagi; Yoshiomi Yoshida; Yasuo Azefu; Hitoshi Tamiaki


Publisher
John Wiley and Sons
Year
2005
Weight
17 KB
Volume
36
Category
Article
ISSN
0931-7597

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✦ Synopsis


Abstract

For Abstract see ChemInform Abstract in Full Text.


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Οͺ Major Me 4 Si ( 1 H) and CDCl 3 ( 13 C, Ξ΄ Ο­ 77.05). Standard correlation techanomer: 1 H NMR (400 MHz, CDCl 3 ): Ξ΄ Ο­ 3.81Οͺ3.92 (m, 4 H, 5 aniques were used for assignments. Οͺ Mass spectra: Varian CH 7 H, 5 b -H, SCH 2 Ph), 3.95Οͺ3.97 (m, 1 H, 4-H), 3.99 (dd, 1 H, 2-H), (EI) and VG Analytical 70-250