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Synthesis of 3,3,4-trimethylpent-1-yne and 2,3,3,8,8,9-hexamethyldeca-4, 6-diyne

✍ Scribed by A. P. Meshcherynakov; L. V. Petrova

Book ID
112494267
Publisher
Springer
Year
1962
Tongue
English
Weight
133 KB
Volume
10
Category
Article
ISSN
1573-9171

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✍ Ritter, Joachim ;Gleiter, Rolf 📂 Article 📅 1997 🏛 John Wiley and Sons 🌐 English ⚖ 610 KB

## Abstract The preparation of __N__,__N__′‐dialkyl‐ and __N__,__N__′‐diaryl‐1,6‐diazacyclodeca‐3,8‐diynes was achieved by reaction of alkyl‐ or arylamines with 1,4‐dihalobut‐2‐yne under dilution conditions in yields of 5–15%. The compounds synthesized by this procedure were the __N__,__N__′‐dimeth