## Abstract Novel 3‐(substituted)‐2,4,8,15‐tetroxa‐3‐phosphadispiro[5.2.5]hexadecane‐3‐oxides **(3‐12)** have been synthesized by cyclization of 1,5‐dioxaspiro[5.5]undecande‐3,3‐dimethanol **(1)** with various substituted aryl phosphorus dichloridates **(2)** in dry toluene‐THF in the presence of t
✦ LIBER ✦
Synthesis of 3-(Substituted)-2,4,8,15-tetroxa-3-phosphadispiro [5.2.2]hexadecane-3-oxides.
✍ Scribed by Y. Hari Babu; N. Ravi Sankar; C. Suresh Reddy; C. Devendranath Reddy
- Publisher
- John Wiley and Sons
- Year
- 2005
- Weight
- 15 KB
- Volume
- 36
- Category
- Article
- ISSN
- 0931-7597
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✦ Synopsis
Abstract
For Abstract see ChemInform Abstract in Full Text.
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## Abstract Syntheses of 2‐aryloxy/2‐chloro ethoxy‐2,3‐dihydro‐5‐benzoyl‐1H‐1,3,2‐benzodiaza‐phosphole 2‐oxides **3a–h** were accomplished by reactions of equimolar quantities of 3,4‐diaminobenzophenone (**1**) with various aryl/chloroethoxy phosphorodichloridates **2a–g** and **2h** in the presenc