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Synthesis of 3-acylmethyl-1,5-dihydrobenzo[e]-2,4-dithiepins and 1,2-di(acylvinylthiomethyl)-4,5-dimethylbenzenes from α-acetylene ketones

✍ Scribed by A. S. Nakhmanovich; R. V. Karnaukhova; V. N. Elokhina; I. D. Kalikhman

Book ID
112346555
Publisher
Springer US
Year
1985
Tongue
English
Weight
215 KB
Volume
21
Category
Article
ISSN
0009-3122

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✍ Vladimir V. Ivanov; Alexandr A. Yurchenko; Alexander N. Chernega; Alexandr M. Pi 📂 Article 📅 2002 🏛 John Wiley and Sons 🌐 English ⚖ 188 KB

## Abstract A number of 4,5‐dihydrobenzo[__e__]imidazo[2,1‐__c__][1,4,2]diazaphosphinine derivatives were prepared by the direct phosphorylation of 1‐(4‐Chlorophenylcarboxamido)‐2‐(1H‐1‐imidazolyl)‐5‐trifluoromethylbenzene in basic medium with phosphorus(III) bromide and dibromophenylphosphine. The