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Synthesis of 2,6-Dioxo-1,2,3,4,5,6-hexahydroindoles by Acid- Catalyzed Cyclization of Acetal-Protected (2,4-Dioxocyclohex-1-yl)acetamides and their Transformation into 5,8,9,10-Tetrahydro-6H-indolo[2,1-a]isoquinolin-9-ones

✍ Scribed by Benard Juma; Muhammad Adeel; Alexander Villinger; Helmut Reinke; Anke Spannenberg; Christine Fischer; Peter Langer


Publisher
John Wiley and Sons
Year
2009
Tongue
English
Weight
254 KB
Volume
351
Category
Article
ISSN
1615-4150

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Two coordination polymers 1 Ο± {[Cd(phen)](C 6 H 8 O 4 ) 3/3 } (1) and 1 Ο± {[Cd(phen)](C 7 H 10 O 4 ) 3/3 } β€’ 2H 2 O (2) were structurally characterized by single crystal X-ray diffraction methods. In 1 (C2/ c (no. 15), a Ο­ 16.169(2) A ˚, b Ο­ 15.485(2) A ˚, c Ο­ 14.044(2) A ˚, Ξ² Ο­ 112.701(8)Β°, U Ο­ 324