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Synthesis of 2,5-disubstituted-3-cyanoindoles

โœ Scribed by Mark A. Bobko; Karen A. Evans; Arun C. Kaura; Leanna E. Shuster; Dai-Shi Su

Book ID
113930251
Publisher
Elsevier Science
Year
2012
Tongue
French
Weight
437 KB
Volume
53
Category
Article
ISSN
0040-4039

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โœ Caroline L. Nesbitt; Christopher S.P. McErlean ๐Ÿ“‚ Article ๐Ÿ“… 2009 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 351 KB

Single enantiomer 2,5-disubstituted-3-oxygenated tetrahydrofurans are synthesized in as little as four steps from a commercially available epoxide. The key steps are homoallylic alcohol epoxidation, palladium-catalysed alkoxy-carbonylation-lactonisation and Mitsunobu inversion. The protocol is appli