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Synthesis of 2,5-Dibromo-1,2,4-triazole by Bromination of 1,2,4-Triazole

✍ Scribed by Doz. Dr. C.-F. Kröger; Dipl.-Chem. H. Frank

Publisher: John Wiley and Sons
Year: 1965
Tongue: English
Weight: 121 KB
Volume: 4
Category: Article
ISSN: 0044-8249
DOI: 10.1002/anie.196504342

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The title compound (C 15 H 12 N 3 OSCl) crystallizes in the monoclinic space group P2 1 /n with a = 11.211( 3), b = 8.106(2), c = 17.494(4) Å, β = 104.49(2)º, V = 1539.2(7) Å 3 , Z = 4, D cal = 1.371 Mg/m 3 at T = 293 K. The structure was solved by direct methods and refined by full-matrix least-squ