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Synthesis of 2,3,5-trihydroxyphenylprop-1-ene and its 4-chloro-, 6-chloro-, and 4,6-dichloro- derivatives

✍ Scribed by Hill, Robert A.; Macaulay, Graham S.; MacLachlan, William S.


Book ID
121466494
Publisher
Royal Society of Chemistry
Year
1987
Weight
893 KB
Category
Article
ISSN
1472-7781

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## Abstract [^14^C] Aniline hydrogen sulphate was acetylated, and the acetanilide obtained was chlorinated with N‐chlorosuccinimide to 2‐chloro, 4‐chloro‐ and 2, 4‐dichloroacet[^14^C] anilide. The labelled 2‐ and 4‐chloroacet[^14^C] anilides were hydrolyzed and treated with aluminium chloride, hydr