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Synthesis of 2,2-functionalized benzo[1,3]dioxoles

✍ Scribed by Nader M. Boshta; Martin Bomkamp; Siegfried R. Waldvogel

Book ID
108282933
Publisher
Elsevier Science
Year
2009
Tongue
French
Weight
668 KB
Volume
65
Category
Article
ISSN
0040-4020

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The title compound, C 24 H 20 O 10 , is centrosymmetric about the central C C bond, indicating that the molecule adopts a trans configuration and that the aromatic rings are parallel to each other. The crystal structure is stabilized by intermolecular C-HÁ Á ÁO interactions.

2-dimethylamino-benzo-1.3-dioxole durch
2-dimethylamino-benzo-1.3-dioxole durch cyclisierung von dimethyl[(2-hydroxy-phenoxy)-methylen]-imoniumchloriden
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Von in 2-Stellung substltulerten Benzo-l.+dloxolen, die im Prlnzlp elner a -. \ Eliminlerung fahig slnd, sind bisher nur wenlge Vertreter bekannt 'I. Wir beschreiben die Darstellung von 2-Dlmethylamino-benzo-1.3-dioxolen 1, die slch