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Synthesis of 2-R-2-(1-Aryl-7,8-Dimethoxy-5H-2,3-Benzodiazepin-4-yl)Acetic Acid Esters in the Eschenmoser Reaction

✍ Scribed by Sizonenko, E. S.; Kobrakov, I. K.; Popov, V. Yu.; Suikov, S. Yu.; Bogza, S. L.

Book ID: 121599934
Publisher: Springer US
Year: 2013
Tongue: English
Weight: 573 KB
Volume: 49
Category: Article
ISSN: 0009-3122
DOI: 10.1007/s10593-013-1384-0

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## Abstract The hydroperoxy endoperoxide **3**, obtained by photooxygenation of isotetralin (= 1,4,5,8‐tetrahydronaphthalene; **1**), was reduced with thiourea, and the resulting intermediate **4** was converted, after acetylation with acetyl chloride, to the interesting, double‐chlorinated acetate