Synthesis of 2-meth ylacetoa cetic ester by the methylation of acetoacetic ester with dimethyl sulfate
✍ Scribed by É. A. Mistryukov
- Book ID
- 112434818
- Publisher
- Springer
- Year
- 1961
- Tongue
- English
- Weight
- 145 KB
- Volume
- 10
- Category
- Article
- ISSN
- 1573-9171
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Whereas condensation of 2-methyl-3-nitrobenzoate esters with dimethylformamide dimethyl acetal gives 5-nitroisocoumarin, analogous condensation with dimethylacetamide dimethyl acetal proceeds via a different route, affording 1-methoxy-3dimethylamino-5-nitronaphthalene in good yield. Extension of the