Synthesis of 2-chloro-2-n-butyl-1,3-dithia-2-stannacyclopentane and the crystal structure of its 1,10-phenanthroline complex
β Scribed by G. Bandoli; U. Casellato; V. Peruzzo; G. Plazzogna
- Publisher
- Elsevier Science
- Year
- 1991
- Tongue
- English
- Weight
- 365 KB
- Volume
- 411
- Category
- Article
- ISSN
- 0022-328X
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## Abstract Two ruthenium complexes [Ru(phen)~2~(mβ36)]^2+^ and [Ru(aphen)~2~(mβ36)]^2+^, indicated as 1 and 2 respectively, which contain a 36βmembered macrocycle incorporating a sterically hindered bipyridine (mβ36), and two 1,10βphenanthroline (phen) or 4β(__p__βanisyl)β1,10βphenanthroline (aphe
Blue crystals of Cu 2 (phen) 2 (H 2 O) 2 (C 5 H 6 O 4 ) 2 were obtained from a CH 3 OHΒ±H 2 O solution containing CuCl 2 , 1,10-phenanthroline (phen), glutaric acid and Na 2 CO 3 . The crystal structure (monoclinic, P2 1 /c (no. 14), a = 10.271(1), b = 10.595(1), c = 15.585(1) A Γ , b = 107.105(3)Β°,
Dark blue plate-like crystals of [Cu 2 (phen) 2 (H 2 O) 2 (OH) 2 ](HCO 3 ) 2 Β΄6 H 2 O were obtained from a CH 3 OHΒ±H 2 O solution containing CuCl 2 , 1,10-phenanthroline (phen), sebacic acid and Na 2 CO 3 . The crystal structure (triclinic, P 1 (no. 2), a = 8.118(1), b = 9.624(1), c = 10.536(1) A Γ