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Synthesis of 2-amino-4,4-bis(trifluoromethyl)-3-cyano-1,4-dihydrobenzo[h]-quinoline

โœ Scribed by K. V. Komarov; N. D. Chkanikov; S. V. Sereda; M. Yu. Antipin; Yu. T. Struchkov; A. F. Kolomiets; A. V. Fokin

Book ID
112448741
Publisher
Springer
Year
1988
Tongue
English
Weight
251 KB
Volume
37
Category
Article
ISSN
1573-9171

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A 1:1 cocrystal of 2,8-bis(trifluorometh
A 1:1 cocrystal of 2,8-bis(trifluoromethyl)quinolin-4-ol and 2,8-bis(trifluoromethyl)quinolin-4(1H)-one
โœ Sarojini, B. K. ;Narayana, B. ;Mayekar, Anil N. ;Yathirajan, H. S. ;Bolte, Micha ๐Ÿ“‚ Article ๐Ÿ“… 2007 ๐Ÿ› International Union of Crystallography ๐ŸŒ English โš– 350 KB

In the title compound, C~11~H~5~F~6~NOยทC~11~H~5~F~6~NO, both molecules (except F and H atoms) are essentially planar (the r.m.s. deviations for all non-H atoms are 0.008 and 0.034โ€…ร… for the alcohol and ketone, respectively). The two molecules are connected by an Oโ€”H...O hydrogen bond. The protonated