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Synthesis of 2-alkyl(aryl)amino-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-d-glucopyrano)[2,1-d]-2-oxazolines and ethyl 2-[3-alkyl(aryl)ureido]-2-deoxy-β-d-glucopyranosides from acetylated 2-[3-alkyl(aryl)ureido]-2-deoxy-d-glucopyranoses

✍ Scribed by Martin Avalos Gonzalez; Pedro Cintas Moreno; Isabel M. Gomez Monterrey; Jose L. Jimenez Requejo; Juan C. Palacios Albarran; Francisca Rebolledo Vicente; Jose Fuentes Mota

Book ID
107725979
Publisher
Elsevier Science
Year
1990
Tongue
English
Weight
467 KB
Volume
197
Category
Article
ISSN
0008-6215

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The crystal and molecular structure of Z-phenyl-(3,4,6- (2) has been determined. The compound crystallises in the space group P2,2,2 with lattice constants 13.4160(3), 37.4931( 14)) and 7.7886( 1) A, and Z = 8. Direct methods were used in the solution. Least squares refined the model with 3213 obse

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The X-ray diffraction analysis of methyl 2,3,6-tri-O-acetyl-2-deoxy-2-[3-(2-phenylethyl)-ureido]-beta-D- glucopyranoside has been performed, establishing that molecules are associated by two types of NH...O hydrogen bonds, N-1-H with carbonyl-oxygen and N-3-H with anomeric oxygen, with N...O distanc