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Synthesis Of 1,5-Benzodiazepine Derivatives

โœ Scribed by Dai-Il, Jung; Tae-wonchoi, Choi; Yun-Young, Kim; In-Shik, Kim; You-Mi, Park; Yong-Gyun, Lee; Doo-Hee, Jung

Book ID
120340231
Publisher
Taylor and Francis Group
Year
1999
Tongue
English
Weight
433 KB
Volume
29
Category
Article
ISSN
0039-7911

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Ytterbium triflate promoted synthesis of
Ytterbium triflate promoted synthesis of 1,5-benzodiazepine derivatives
โœ Massimo Curini; Francesco Epifano; Maria C Marcotullio; Ornelio Rosati ๐Ÿ“‚ Article ๐Ÿ“… 2001 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 82 KB

2,3-Dihydro-1H-1,5 benzodiazepines have been synthetized in very good yield in solvent-free conditions from o-phenylendiamine and ketones in the presence of Yb(OTf) 3 as catalyst. The method is applicable to both cyclic or acyclic ketones without significant differences.