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Synthesis of 1,4-Diazepin-5-ones under Microwave Irradiation and Their Reduction Products.

✍ Scribed by Nicolas Wlodarczyk; Pauline Gilleron; Regis Millet; Raymond Houssin; Jean-Pierre Henichart


Book ID
102002848
Publisher
John Wiley and Sons
Year
2007
Weight
21 KB
Volume
38
Category
Article
ISSN
0931-7597

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## Abstract magnified image Novel 11‐amino‐6‐aryl‐6,7‐dihydroindeno[1,2‐__e__] pyrimido[4,5‐__b__][1,4]diazepin‐5(5a__H__)‐ones 4a‐f were prepared regioselectively by the tricomponent reaction of 4,5,6‐triaminopyrimidine 1, 1,3‐indandione 2 and aromatic aldehydes 3a‐f. The bicomponent approach, us