SYNTHESIS OF [a-14C]-BENZYLGUANIDINE Muthiah N. I n b a s e k a r a n , Thomas J . Mangner and Donald M. Wieland D i r i s i o n of N u c l e a r Medicine Ann Arbor, Michigan, 48109. The l l n i v e r s i t y of Michigan Medical C e n t e r SUEl MAKY [ ~~~C ] -b e n z y l g u a n i d i n e (1) h a v
✦ LIBER ✦
Synthesis of 14-deoxy-14α-strophanthidin
✍ Scribed by Pavel Kočovský
- Publisher
- Elsevier Science
- Year
- 1980
- Tongue
- French
- Weight
- 199 KB
- Volume
- 21
- Category
- Article
- ISSN
- 0040-4039
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## Abstract We describe, herein, the first synthesis of isomerically pure title compound (__6__) at high specific activity. This required the development of a convenient, regiospecific synthesis of the Δ^8(9)^‐15‐ketone (__15__) and subsequent alkylation with methyl‐[^3^H~3~] iodide. A key step in