Synthesis of 1,2,6-Tris(2-cyanoethoxy)hexane
✍ Scribed by Froberger, C. F.; McEwen, D. J.
- Book ID
- 126277029
- Publisher
- American Chemical Society
- Year
- 1962
- Tongue
- English
- Weight
- 270 KB
- Volume
- 27
- Category
- Article
- ISSN
- 0022-3263
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## Abstract MgO/ZrO~2~ catalyst was prepared for the synthesis of 1,6‐dicarbamate hexane (HDC) using dimethyl carbonate (DMC) and 1,6‐diamine hexane (HDA) as raw materials. When the catalyst is calcined at 600 °C and MgO load is 6 wt%, the catalyst exhibits better activity. When the concentration o
The title compound, C 24 H 36 , crystallizes with two independent but very similar molecules in the asymmetric unit. The ring torsion angles about the double bonds are ca 13 ; the ring sp 2 bond angles at the three radialene-type junctions are ca 110 .