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Synthesis of 11Z-9-demethyl-9-((3-indolyl)methyl)retinal

✍ Scribed by Akimori Wada; Naoko Fujioka; Masayoshi Ito

Publisher: Journal of Heterocyclic Chemistry
Year: 2001
Tongue: English
Weight: 76 KB
Volume: 38
Category: Article
ISSN: 0022-152X
DOI: 10.1002/jhet.5570380138

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✦ Synopsis

Abstract

A convenient synthesis of 11Z‐9‐demethyl‐9‐((3‐indolyl)methyl)retinal, which has an amino acid residue of tryptophan at the 9 position in retinal, is described using a tricarbonyliron complex.

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## Abstract (±) 3‐(6‐Nitro‐2‐quinolinyl)‐[9‐methyl‐^11^C]‐3,9‐diazabicyclo‐[4.2.1]‐nonane ([^11^C‐methyl]NS 4194), a selective serotonin reuptake inhibitor (SSRI), was synthesised within 35 min after end of bombardment with a radiochemical purity >98%. It had a decay‐corrected radiochemical yield o