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Synthesis of 1-Substituted Thymines

✍ Scribed by Smith, Robert; Binkley, Stephen

Book ID
118239556
Publisher
American Chemical Society
Year
1959
Tongue
English
Weight
426 KB
Volume
24
Category
Article
ISSN
0022-3263

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## Abstract Free radicals generated by reaction of protected methyl 2,3‐ dideoxy‐3‐iodopentofuranosides 2, 3, and 9 with tributyltin hydride in the presence of a radical initiator (AIBN) were treated with acrolein to give methyl 2,3‐dideoxy‐3‐(3‐oxopropyl)pentofuranosides 4 and 5. Reduction of 5 wi