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Synthesis of 1′-Methylspiro [3H-naphtho[2,1-b]-pyran-3,2′(1,2-dihydroquinoline)]

✍ Scribed by Dr. C. Schiele; H. O. Kalinowski


Publisher
John Wiley and Sons
Year
1966
Tongue
English
Weight
103 KB
Volume
5
Category
Article
ISSN
0044-8249

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The 1H and 13C NMR resonances of four 3H-naphtho[2,1-b]pyrans were completely and unambiguously assigned by a combination of homonuclear (gs-COSY), 1H-detected heteronuclear one-bond (gs-HMQC) and long-range (gs-HMBC) gradient-selected correlation experiments.