Synthesis of 1-Methyl- and 1,6-Dimethyl-3-methoxy-4-isopropylnaphthalene
✍ Scribed by TALUKDAR, P. B.
- Book ID
- 126805080
- Publisher
- American Chemical Society
- Year
- 1956
- Tongue
- English
- Weight
- 395 KB
- Volume
- 21
- Category
- Article
- ISSN
- 0022-3263
No coin nor oath required. For personal study only.
📜 SIMILAR VOLUMES
In the title compound, C 14 H 15 NO 5 , the 1,3-dioxane-4,6-dione ring exhibits a half-chair conformation. The amino H atom has one intra-and one intermolecular contact to carbonyl O atoms, with OÁ Á ÁH distances of 2.11 (2) and 2.31 (2) A ˚.
Single-crystal X-ray study T = 183 K Mean '(C±C) = 0.002 A Ê Disorder in main residue R factor = 0.049 wR factor = 0.144 Data-to-parameter ratio = 16.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 100 K Mean '(C±C) = 0.002 A Ê R factor = 0.041 wR factor = 0.116 Data-to-parameter ratio = 14.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.