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Synthesis of 1-Fluoro-2-amino-1,3-cyclohexadienes and 1-Fluorobicyclo[2.2.2]octan-2-ones

✍ Scribed by Heike Pick-Schliebs; Paul Margaretha

Publisher
John Wiley and Sons
Year
1987
Tongue
German
Weight
171 KB
Volume
70
Category
Article
ISSN
0018-019X

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✦ Synopsis

In CDCI,. ') Values of J(C,F) given b, Signals of amino component not indicated.

d, 6b/7b (3 : 1 mixture).

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## Abstract The reaction of the 4,4‐dialkylated 2‐cyclohexenones **1** or **2** with a twofold excess of a secondary amine **3** affords the 2‐amino‐1,3‐cyclohexadienes **4** and **5**, respectively. Irradiation (λ ≧ 300 nm) of the morpholino derivative **4a** yields a mixture of the isomeric 3‐mor

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## Abstract Die bislang unbekannten 1,2,3‐Cyclohexantrione **5** können in Form ihrer Chlorhydrine **2** oder deren Ester **4** leicht in die entsprechenden 2,6‐Dihydroxy‐2,5‐cyclohexadien‐1‐one **6** oder deren Ester **8** umgelagert werden.