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Synthesis of 1- ethylsulphonylnaphthalene-4-(35S)-sulphonamide, a murine bladder carcinogen

✍ Scribed by R. Turner; H. G. Dean

Book ID: 102373956
Publisher: John Wiley and Sons
Year: 1969
Tongue: French
Weight: 184 KB
Volume: 5
Category: Article
ISSN: 0022-2135
DOI: 10.1002/jlcr.2590050208

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✦ Synopsis

Diazotisation of 1-ethylsulphonyl-4-naphthylamine followed by treatment with sulphur dioxide-35s in acetic acid and then cupric chloride gave l-ethyl~ulphonylnaphthalene-4-(~~S)-sulphonyl chloride. This gave the title compound by reaction with aqueous ammonia. Total time required was three days.

Synthesis of l-Ethyl~ulphonylnaphthalene-4-(~~S) -sulphonamide.

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