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SYNTHESIS OF 1-AZIDO-1, 3-BUTADIENES

✍ Scribed by Isomura, Kazuakl; Okada, Masato; Ogawa, Hideaki; Ichiki, Makoto; Taniguchi, Hiroshi

Book ID
120346530
Publisher
Taylor and Francis Group
Year
1972
Tongue
English
Weight
225 KB
Volume
4
Category
Article
ISSN
0030-4948

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## Abstract Iodine azide adds to cyclohexene in acetonitrile or 4:1 methylene chloride/acetonitrile to give __trans__‐1‐azido‐2‐iodocyclohexane. In methylene chloride this reaction gives a mixture of the __cis__‐and __trans__‐iodoazides owing to competing radical addition. Iodine azide adds to 1‐he