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Synthesis of 1-, 2-, and 6-Azulenethiols

✍ Scribed by Toyonobu Asao; Shunji Ito; Noboru Morita

Book ID
104244972
Publisher
Elsevier Science
Year
1989
Tongue
French
Weight
164 KB
Volume
30
Category
Article
ISSN
0040-4039

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✦ Synopsis

l-Azulenethiol was synthesized by reductive cleavage of di-l-azulyl disulfide, and 2-and 6-azulenethiols were synthesized by the conversion of the corresponding hydroxyl group to mercapto group via dimethylthiocarbamates.

Several reports of the attachment of sulfur atom to azulene nucleus have been found in the literature in the chemistry of azulene. I) IIowever, no report on the synthesis of azulenethiols has been appeared, although some efforts have been devoted; 2) acid or base catalyzed hydrolysis

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