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Synthesis, mass spectrometry and NMR spectroscopy studies of the (CH3)2 In(C2H5) system: X-ray crystal structure of a diphosphine-bridged complex

✍ Scribed by P. Visonà; F. Benetollo; G. Rossetto; P. Zanella; P. Traldi

Publisher: Elsevier Science
Year: 1996
Tongue: English
Weight: 660 KB
Volume: 511
Category: Article
ISSN: 0022-328X
DOI: 10.1016/0022-328x(95)05976-v

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## Abstract A comprehensive ^31^P solid‐state NMR study of Ru(η^1^‐Ph~2~PCH~2~CH~2~OCH~3~)~2~(η^2^‐en)Cl~2~ (en = ethylenediamine) (1), by 1D (contact time variation, inversion–recovery, SPARTAN) and 2D techniques (homonuclear __J__‐resolved, SECSY) indicated that the crystal structure of 1 should