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Synthesis, Magnetism, and Crystal Structure of Li2Fe[(PO4)(HPO4)] and Its Hydrogen Position Refinement.

โœ Scribed by Jin-Xiao Mi; Horst Borrmann; Hui Zhang; Ya-Xi Huang; Walter Schnelle; Jing-Tai Zhao; Ruediger Kniep


Publisher
John Wiley and Sons
Year
2004
Weight
13 KB
Volume
35
Category
Article
ISSN
0931-7597

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Preparation and Crystal Structure of Sod
โœ N. Anissimova; A. Ilyukhin; N. Chudinova; R. Glaum ๐Ÿ“‚ Article ๐Ÿ“… 1998 ๐Ÿ› John Wiley and Sons ๐ŸŒ German โš– 137 KB ๐Ÿ‘ 2 views

Single crystals of sodium iron hydrogen phosphate, NaFe(HPO 4 )(H 2 PO 4 ) 2 ยดH2 O, were prepared hydrothermally by heating a mixture of Fe 2 O 3 , H 3 PO 4 and Na 2 CO 3 with a small amount of water. It crystallizes orthorhombic (Pbcn (Nยฐ60), Z = 8, a = 872.91( 7), b = 1249.54(8), c = 1894.4(1) pm)