Synthesis, Structure, and Physical Prope
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Mohamedally Kurmoo; Mario Bonamico; Carlo Bellitto; Vincenzo Fares; Fulvio Feder
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Article
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1998
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John Wiley and Sons
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English
⚖ 266 KB
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Bromohexyl)-3¢,4¢-ethylenedioxy)-2,2¢-bithiophene (3): Into a roundbottomed flask were introduced EDOT (5.9 g, 41.4 mmol) and 150 mL of tetrahydrofuran (THF). The mixture was cooled to ±40 C and butyllithium, 2.5 M in hexanes (19 mL, 47.5 mmol), was added rapidly. After 1 h stirring, tributyltin chl