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Synthesis, Crystal Structures and Physical Properties of TTF-Based Conducting Charge Transfer Salts with Anions Containing Selenocyanate Ligands

✍ Scribed by Scott S. Turner; Delphine Le Pévelen; Peter Day; Keith Prout

Publisher: Elsevier Science
Year: 2002
Tongue: English
Weight: 349 KB
Volume: 168
Category: Article
ISSN: 0022-4596
DOI: 10.1006/jssc.2002.9754

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✦ Synopsis

Three new charge transfer salts of tetrathiafulvalene (TTF)based donors with selenocyanate-metal complex anions have been synthesized. The salts have been characterized as BEDT-TTF 4 [Cr(NCSe) 6 ] . CH 2 Cl 2 , II, TTF 3 [Cr(NCSe) 4 phen] 2 , III and BEDT-TTF 2 [Cr(NCSe) 4 phen] Á CH 2 Cl 2 , IV, where phen=1,10 0phenanthroline and BEDT-TTF=bis(ethylenedithio)tetrathiafulvalene. At 120 K, II crystallizes in the P2 1 /m space group with a ¼ 10:454(1),

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