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Synthesis, crystal structure of some new 2-(4-methylbenzoylimino)-3-aryl-4-methyl-1,3-thiazolines

✍ Scribed by Aamer Saeed; Masood Parvez

Publisher: Journal of Heterocyclic Chemistry
Year: 2006
Tongue: English
Weight: 109 KB
Volume: 43
Category: Article
ISSN: 0022-152X
DOI: 10.1002/jhet.5570430431

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✦ Synopsis

Abstract

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An efficient, straightforward synthesis of some new 2‐(4‐methylbenzoylimino)‐3‐aryl‐4‐methyl‐1,3‐thiazolines (2a‐i) is described. The methodology involves the cyclization of 1‐(4‐methylbenzoyl)‐3‐arylthioureas with acetone in the presence of bromine and triethylamine. The structures were confirmed by spectroscopic data, elemental analyses and in one case (2i) by the single crystal X‐ray diffraction data.

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