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Synthesis, crystal structure, and thermal analysis of hexahydrogen dodecavanadate of composition [NH3· H2O]6· H6[Ca4V12O40] · 6H2O

✍ Scribed by A. F. Stepnova, A. V. Oreshkina, G. Z. Kaziev, S. Holguin Quinones, A. I. Stash

Book ID
114990014
Publisher
SP MAIK Nauka/Interperiodica
Year
2012
Tongue
English
Weight
233 KB
Volume
57
Category
Article
ISSN
0036-0236

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✍ H.D. Lutz; R. Nagel; S.A. Mason; A. Müller; H. Bögge; E. Krickemeyer 📂 Article 📅 2002 🏛 Elsevier Science 🌐 English ⚖ 446 KB

The crystal structure of (NH 4 ) 21 [H 3 Mo 57 V 6 (NO) 6 O 183 (H 2 O) 18 ] . 53 H 2 O, a supramolecular heteropoly cluster compound (space group P6 3 /mmc, Z=2, final R1=0.1302 (I42r(I)) for 1745 unique reflections), was redetermined by single-crystal neutron diffraction studies at 20 K. The X-ray