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Synthesis, crystal structure and TEM study of the new hollandite-type Ba∼8/7Mo8O16

✍ Scribed by N. Barrier; P. Gougeon; R. Retoux

Book ID
117619509
Publisher
Elsevier Science
Year
2001
Tongue
English
Weight
1000 KB
Volume
317-318
Category
Article
ISSN
0925-8388

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✍ J. Tortelier; W.H. McCarroll; P. Gougeon 📂 Article 📅 1998 🏛 Elsevier Science 🌐 English ⚖ 363 KB

Single crystals of NdMo 6 O 12 were prepared by fused-salt electrolysis at 960°°C from a melt of Rb 2 MoO 4 , MoO 3 , and Nd 2 O 3 having the molar ratio 8.4 : 5 : 1. The compound crystallizes in the tetragonal space group I4/m with a ‫؍‬ 9.8988(2) A s , c ‫؍‬ 8.6434(5) A s , V ‫؍‬ 846.93(5) A s 3 ,