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Synthesis, Crystal Structure and Properties of a New One-Dimensional 3d-4f Compound

✍ Scribed by Zhao Qi-Hua; Qing-Hua Wang; Rui-Bin Fang; Zhi-Da Chen

Publisher: John Wiley and Sons
Year: 2010
Tongue: English
Weight: 303 KB
Volume: 22
Category: Article
ISSN: 0256-7660
DOI: 10.1002/cjoc.20040220310

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✦ Synopsis

A new heterornetallic complex K2[(Eu(H20)4}~{Fen(bipyX~)4] 9H20 CH3OH [bipy=2,2'-bipyridine] was synthesized. The compound has been characterized by X-ray structure analysis, elemental analyses, IR spectrum, TGA thennogram and magnetic susceptibility. The complex consists of novel one-dimensional ladder structure. The crystal belongs to monoclinic system with a space group P2,lc. a =1.3946(4) nm, b=2.0450(6) nm. c=2.9722(8) nm. /3=99.W(5)O, V=8.372(4) nm3, 2=4. D,= 1.562 g -~r n -~.

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