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Synthesis, crystal structure, and NMR investigation of methyl α,α-dimethyl acetate-substituted π-allylpalladium complexes

✍ Scribed by Ido Schwarz; Jörg Rust; Christian W Lehmann; Manfred Braun

Book ID
108346666
Publisher
Elsevier Science
Year
2000
Tongue
English
Weight
207 KB
Volume
605
Category
Article
ISSN
0022-328X

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✍ Yan-Long Qian; Xin-Rong Qin; Ji-Ling Huang; Albert Sun-Chi Chan; Shou-Shan Chen; 📂 Article 📅 2010 🏛 John Wiley and Sons 🌐 English ⚖ 292 KB

## Abstract The syntheses of a series of l‐methyl‐3‐aryl‐substituted titanocene and zirconocene dichlorides are reported. These complexes are synthesized by the reaction of 2‐ and 3‐methyl‐6, 6‐dimethylfulvenes (1:4) with aryllithium, followed by the reaction with TiCl~4~·2THF, ZrCl~4~ and (CpTiCl~