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Synthesis, Crystal Structure and Magnetic Properties of Novel Three-dimensional Frameworks [Mn(PDC)H2O]n

✍ Scribed by En-Jun GAO; Xiao-Fu GU; Ya-Guang SUN; Hong-Xi YIN; Qiong WU; Lei LIU; Ming-Chang ZHU; Wan-Zhong ZHANG

Publisher: John Wiley and Sons
Year: 2008
Tongue: English
Weight: 115 KB
Volume: 26
Category: Article
ISSN: 0256-7660
DOI: 10.1002/cjoc.200890381

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✦ Synopsis

A novel coordination polymer, [Mn(PDC)H 2 O] n (1) (H 2 PDC＝pyridine-2,3-dicarboxylic acid), has been hydrothermally synthesized and characterized by elemental analysis, IR and single crystal X-ray diffraction. X-ray single crystal structural analyses revealed that two-dimensional frameworks were formed, and further assembled into a three-dimensional supramolecular structure bridged by PDC ligands. Moreover, the magnetic study of complex 1 shows weak antiferromagnetic interaction between the neighboring Mn(II) centers within the chains and even weak ferromagnetic interactions between the Mn(II) centers in different chains.

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