Synthesis, crystal structure and DFT studies of N-(4-acetyl-5,5-dimethyl-4,5-dihydro-1,3,4-thiadiazol-2-yl)acetamide
β Scribed by Gautam, P.; Gautam, D.; Chaudhary, R. P.
- Book ID
- 121584122
- Publisher
- SP MAIK Nauka/Interperiodica
- Year
- 2013
- Tongue
- English
- Weight
- 216 KB
- Volume
- 58
- Category
- Article
- ISSN
- 1063-7745
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π SIMILAR VOLUMES
## Abstract via condensation of thiosemicarbazides (V) with Ac~2~O (10 examples)
In the title compound, C 12 H 10 F 3 N 3 O 2 S, the molecules are linked into two-dimensional networks parallel to (110) through a mixture ofstacking and N-HΓ Γ ΓN hydrogenbond interactions.
The synthesis of new 1,3,4-thiadiazoline derived from 3-methyl-2,6-diphenyltetrahydropyran-4-one, via the corresponding thiosemicarbazone, is described. The synthesis, spectral characterization and crystal structure of 5-spiro-1,3,4-thiadiazoline of 2,6-diphenyl-3-methylpyran is reported. Spectral t