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Synthesis, Crystal Structure and Characterization of a Mixed-Valence Keggin-Structural 12-Molybdophosphoric Acid Compound: NH4(C4N2H12)(C2N2H10)2[Mo4VMo8VIPO40]·2H2O

✍ Scribed by Zhi-biao Hu, Ze-hai Qiu, Wu-hua Chen

Book ID
120692550
Publisher
Springer
Year
2013
Tongue
English
Weight
497 KB
Volume
24
Category
Article
ISSN
1040-7278

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Hydrothermal Synthesis and Characterizat
Hydrothermal Synthesis and Characterization of Two Mixed Valence Piperazine–Vanadium Phosphates: (C4H12N2)(H3O)[(VOPO4)4(H2O)H2PO4]·3H2O and (C4H12N2)[(VO)(VO2)2(H2O)(PO4)2]
✍ Junghwan Do; Ranko P. Bontchev; Allan J. Jacobson 📂 Article 📅 2000 🏛 Elsevier Science 🌐 English ⚖ 488 KB

Two new phases, (C 4 H 12 N 2 )(H 3 O)[(VOPO 4 ) 4 (H 2 O)H 2 PO 4 ] ' 3H 2 O (1) and (C 4 H 12 N 2 )[(VO)(VO 2 ) 2 (H 2 O)(PO 4 ) 2 ] (2) have been synthesized hydrothermally and characterized by single crystal X-ray di4raction, thermogravimetric analysis, and magnetic susceptibility. Compound 1 ha