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Synthesis, Crystal Structure, and Application of the Oxonium Acid [H(OEt 2 ) 2 ] + [B(C 6 F 5 ) 4 ] -

✍ Scribed by Jutzi, Peter; Müller, Christian; Stammler, Anja; Stammler, Hans-Georg

Book ID: 120767569
Publisher: American Chemical Society
Year: 2000
Tongue: English
Weight: 50 KB
Volume: 19
Category: Article
ISSN: 0276-7333
DOI: 10.1021/om990612w

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## Abstract Ph~3~SnN(SiMe~3~)~2~ (1) was prepared in good yields by reaction of [{NaN(SiMe~3~)~2~}~2~·THF] (2) with Ph~3~SnF. Treatment of 1 with [H(OEt~2~)~2~][H~2~N{B(C~6~F~5~)~3~}~2~] (4) in dichloromethane afforded the stannylium cation [Ph~3~Sn(OEt~2~)][H~2~N{B(C~6~F~5~)~3~}~2~] (5), which was