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Synthesis, crystal growth, spectral, thermal and optical properties of acenaphthene picrate

✍ Scribed by A. Chandramohan; R. Bharathikannan; M. A. Kandhaswamy; J. Chandrasekaran; V. Kandavelu

Publisher
John Wiley and Sons
Year
2008
Tongue
English
Weight
131 KB
Volume
43
Category
Article
ISSN
0232-1300

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✦ Synopsis

Abstract

The crystalline material of acenaphthene picrate (ACP) was synthesized and the single crystals of the title compound grown by slow evaporation solution growth technique. The solubility of the complex compound was estimated using different solvents as chloroform, ethanol, (1:1) chloroform ‐ acetone mixture. The material was characterized through elemental analysis; powder XRD, NMR and FTIR techniques. The various planes of reflection have been identified from the XRD powder pattern. The formation of the charge transfer complex was confirmed by UV‐VIS spectroscopy. The thermal stability of the crystals was studied using TG/DTA analyses techniques. The second harmonic generation (SHG) of the material was confirmed by using Nd: YAG laser. (Β© 2007 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim)

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