Synthesis, characterization, thermal, and redox properties of a vic -dioxime and its metal complexes
✍ Scribed by Uçar, Asuman; Devecı, Pervın; Taner, Bılge; Findik, Mükerrem; Bereket, Soner; Özcan, Emıne; Osman Solak, Alı
- Book ID
- 126804431
- Publisher
- Taylor and Francis Group
- Year
- 2010
- Tongue
- English
- Weight
- 258 KB
- Volume
- 63
- Category
- Article
- ISSN
- 0095-8972
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## Abstract Nickel(II) complexes with three new vic‐dioxime reagents, N‐(ethyl‐4‐amino‐1‐piperidine carboxylate)phenylglyoxime (L~1~H~2~), N‐(ethyl‐4‐amino‐1‐piperidine carboxylate)glyoxime (L~2~H~2~) and N,N′‐bis(ethyl‐4‐amino‐1‐piperidine carboxylate)glyoxime (L~3~H~2~), have been prepared. Monon
## Abstract A new vic-dioxime ligand, N,N′-bis(aminopyreneglyoxime) (LH2), and its copper(II), nickel(II) and cobalt(II) metal complexes were synthesized and characterized by elemental analyses, IR, UVVIS and 1H and 13C NMR spectra (for the ligand). Mononuclear complexes were synthesized by a react