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Synthesis, characterization and hypergolicity of aliphatic furfurylidene ketones with red fuming nitric acid as oxidizer

✍ Scribed by S.G. Kulkarni; S.P. Panda

Publisher: Elsevier Science
Year: 1981
Tongue: English
Weight: 355 KB
Volume: 40
Category: Article
ISSN: 0010-2180
DOI: 10.1016/0010-2180(81)90107-3

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✦ Synopsis

Syntheses of a few aliphatic furfurylidene ketones, a phenylhydrazone, and a N,N-dimethylhydrazone are reported. The compounds are characterized by their IR and NMR spectra. The ignition delay (ID) values of the compounds with RFNA are measured with and without polymerization and oxidation catalysts. It is noted that the ID values of aliphatic furfurylidene ketones with RFNA can be most effectively decreased by using H2SO 4 as catalyst. Formation of a N,N-dimethylhydrazone derivative is also useful to achieve the same purpose.

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